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equipment:edwards-306:start [2026/04/30 18:32] – [Principles of operation] q3kequipment:edwards-306:start [2026/07/18 22:09] (current) q3k
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 ====== Edwards AUTO 306 Coating System ====== ====== Edwards AUTO 306 Coating System ======
-{{:equipment:edwards-306:20260401_coating-systems-overview.jpg?700|}}+{{:equipment:edwards-306:20260401_coating-systems-overview-with-labels.jpg?700|}}
  
 Multi-process PVD system consisting of two Edwards AUTO 306 coaters and a control cabinet. Multi-process PVD system consisting of two Edwards AUTO 306 coaters and a control cabinet.
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 **Sputter:** **Sputter:**
  
-Needs Argon and refurbishing / bringup.+First sputter experiments were successful, process being tuned and MFC contro system is being built
  
 **Coater:** **Coater:**
  
-Thermal evaporation works, e-beam needs bringup. Film thickness monitor needs a new crystal.+Working.
  
 ===== Resources ===== ===== Resources =====
  
   * [[equipment:edwards-306:log|Lab Notebook for the Coating System]]   * [[equipment:edwards-306:log|Lab Notebook for the Coating System]]
-  * [[https://git.fa-fo.de/fafo/edwards-auto-306/raw/branch/main/manuals/AUTO%20306%20Vacuum%20Coater%20-%20Volume%201%20-%20Installation%20and%20Maintenance%20Instructions.pdf|Edwards AUTO 306 - Volume 1 - Installation and Maintenance Instructions]] +  * Documentation 
-  * [[https://git.fa-fo.de/fafo/edwards-auto-306/raw/branch/main/manuals/AUTO%20306%20Vacuum%20Coater%20-%20Volume%202%20-%20Operating%20Instructions.pdf|Edwards AUTO 306 - Volume 2 - Operating Instructions]] +    * [[https://git.fa-fo.de/fafo/edwards-auto-306/raw/branch/main/manuals/AUTO%20306%20Vacuum%20Coater%20-%20Volume%201%20-%20Installation%20and%20Maintenance%20Instructions.pdf|Edwards AUTO 306 - Volume 1 - Installation and Maintenance Instructions]] 
-  * [[https://git.fa-fo.de/fafo/edwards-auto-306/raw/branch/main/manuals/EXC%20Turbomolecular%20Pump%20Controllers.pdf|Edwards - Turbomolecular Pump Controller Manual]] +    * [[https://git.fa-fo.de/fafo/edwards-auto-306/raw/branch/main/manuals/AUTO%20306%20Vacuum%20Coater%20-%20Volume%202%20-%20Operating%20Instructions.pdf|Edwards AUTO 306 - Volume 2 - Operating Instructions]] 
-  * Techtree: [[https://git.fa-fo.de/fafo/techtree/issues/56|PVD: Thermal Evaporation]] [[https://git.fa-fo.de/fafo/techtree/issues/37|PVD: Sputtering]]+    * [[https://git.fa-fo.de/fafo/edwards-auto-306/raw/branch/main/manuals/EXC%20Turbomolecular%20Pump%20Controllers.pdf|Edwards - Turbomolecular Pump Controller Manual]] 
 +  * Techtree: 
 +    * [[https://git.fa-fo.de/fafo/techtree/issues/56|PVD: Thermal Evaporation]] 
 +    * [[https://git.fa-fo.de/fafo/techtree/issues/37|PVD: Sputtering]] 
 +    * [[https://git.fa-fo.de/fafo/techtree/issues/122|E-Beam PVD]]
  
-{{:equipment:edwards-306:edwards-306-evaporator-panel.png?direct&400|}} 
  
 ===== Standard Operating Procedure ===== ===== Standard Operating Procedure =====
 +{{:equipment:edwards-306:edwards-306-evaporator-panel.png?direct&400|}}
  
 Currently written for the thermal evap unit, should be unified with the sputter unit as it is brought up. Currently written for the thermal evap unit, should be unified with the sputter unit as it is brought up.
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   * **Reset**: in case of failure (timeout, power failure, etc.), acknowledge the fault   * **Reset**: in case of failure (timeout, power failure, etc.), acknowledge the fault
   * **Cycle**: Perform the process above reaching an ultra high vacuum   * **Cycle**: Perform the process above reaching an ultra high vacuum
-  * **Process**: Same as 'cycle', but when an ultimate pressure is reached the chamber seals (the high vacuum valve is closed) and the process can perform a plasma cleaning step+  * **Process**: Same as 'cycle', but when an ultimate pressure is reached the chamber seals (the high vacuum valve is closed) and the user can perform a plasma cleaning step
   * **Seal**: Isolate the chamber from the rest of the system. Usually a prerequisite to then stop or vent the system.   * **Seal**: Isolate the chamber from the rest of the system. Usually a prerequisite to then stop or vent the system.
   * **Stop**: Perform a shutdown process: spin down the turbo and turn off the roughing pump.   * **Stop**: Perform a shutdown process: spin down the turbo and turn off the roughing pump.
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   - Insert sample, and check that shutter actuates when 'SS1' is pressed. If not, manually actuate it a few times and then it should get unstuck.   - Insert sample, and check that shutter actuates when 'SS1' is pressed. If not, manually actuate it a few times and then it should get unstuck.
   - Press 'cycle' after inserting sample.   - Press 'cycle' after inserting sample.
 +
 +==== Plasma Cleaning ====
 +
 +  - Load sample
 +  - Press 'process'.
 +  - Wait until 'fine pumping' is reached (TODO: set thresholds correctly)
 +  - Press 'seal'.
 +  - Select the 'chamber' readout on the vacuum controller with the up/down arrows.
 +  - Open the vent butterfly valve (below chamber), and then slowly open needle valve until pressure starts rising.
 +  - Close valves when pressure reaches around 1e-1 mbar. If overshot, restart process.
 +  - Set LT/0/HT selector to HT, slowly bring up power knob until plasma starts in the chamber and current flows.
 +  - Tweak needle valve and power until a stable plasma is achieved that fills up as much of the chamber as possible.
 +  - Manual recommends running plasma cleaning for 20 minutes for every loaded sample before coating it. No experiments have been performed to confirm whether this actually helps with coating.
  
 ==== Simple Coating ==== ==== Simple Coating ====
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   - Turn off power at rack unit.   - Turn off power at rack unit.
  
 +===== Sputter coater MFCs =====
 +
 +Channel 1: 100SCCM Ar. Channel 2: 100SCCM N2.
 +
 +Pinout:
 +
 +  * Pin 2: Control 0-10V (0-100% of rated flow).
 +  * Pin 4: Output 0-10V (feedback from control).
 +  * Pin 5: shield
 +  * Pin 6: +15V
 +  * Pin 7: test output (unknown)
 +  * Pin 8: common/GND
 +  * Pin 9: -15V
  
 +Currently controlled by lab PSUs. Modbus integration is WIP.